example solution
Flex

High throughput materials synthesis and crystallization with online XRD

FLEX ISYNTH for materials synthesis and crystallization with online / offline XRD
Automated, parallel materials library synthesis (e.g. MOFs, perovskites) and crystallization optimization (e.g. active ingredients) with online benchtop XRD.
Overview

Chemspeed's solution

Materials discovery is driven more and more by the demand for innovative materials which involves diversity and novel routes, meaning more and more experiments typically with the same resources. 

Chemspeed’s fully automated, integrated FLEX ISYNTH stands for a flexible, modular, and uncompromising automated solution that:

Unlocks the chemical space via faster, better, virtually unrestricted “off-road” chemistry investigation of the reaction space, reagent space and materials space.

Chemspeed’s ISYNTH deck modularity provides unrivalled versatility to execute and perform a variety of synthesis workflows in a fully automated fashion, including reaction preparation, multistep synthesis, work-up, purification, analysis and product transfer to storage.

Enhances your efficiency and productivity by a factor of up to 100.

Benefits

Powerful advantages

  • Fully automated, integrated reaction preparation, synthesis, work-up, analysis, output to storage vials for solid- and liquid-phase synthesis as well as reaction screening.
  • Easy-to-use disposable multi-functional, high-precision glass reactor arrays, available reaction scales from μL to mL.
  • Glass reactor arrays with screwless and self-sealing opening / closing, mixing by shaking (up to 1'000 rpm), heating (up to 150°C) and cooling (-20°C), refluxing, vacuum, inertization, evaporation, L/L extraction, filtration, solid-phase extraction, crystallization and drying.
  • Proprietary robotic tool exchange.
  • Gravimetric solid handling from μg to g.
  • Gravimetric liquid handling from mg to g / μL to mL.
  • Chemistry proven liquid handling with e.g. pH, filtration, heated needle extension.
  • Throughput, e.g. 24 / 48 / 96 / ... parallel reactions per run based.
  • Sampling and various integrated analytics such as benchtop online NMR, HPLC (MS), UPLC (MS), GC (MS), UV-VIS, NIR / MIR / DLS measurement cell.
  • Ventilated hood for safety and conditioned operation.
  • AUTOSUITE SOFTWARE - drag & drop experimentation with easy interface (e.g. python custom device) to e.g. LIMS, ELN, data analysis, AI / ML closed loop.
  • Integrated online benchtop XRD such as Bruker D6 Phaser, Malvern Aeris, incl. XRD device, sample handover station, software and hardware integration
Software

AUTOSUITE

Chemspeed’s AUTOSUITE software packages execute and control all modules in every solution. They control all Chemspeed robotic platforms and any other integrated 3rd-party software and hardware.

Explore AUTOSUITE
Chemspeed AutoSuite Software laptop screen
Automate and digitalize your laboratory with Chemspeed.