example solution
Swing

High output (mixed) oxide synthesis by pH-controlled precipitation, ion exchange, sol-gel processes

MULTIPLANT / AUTOPLANT PRECIP for pH controlled precipitation
End-to-end automated (mixed) oxide synthesis by pH-controlled precipitation, ion exchange, sol-gel processes, incl. reaction preparation, synthesis, washing, drying for e.g. refinery catalysts, adsorbents, cathode materials.
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Overview

Chemspeed's solution

The leading technology in overhead gravimetric dispensing / dosing (patented) combined with our reactor and process excellence, and our user-friendly software, allow you to accelerate, standardize and digitalize your (mixed) oxide synthesis workflows (precipitation, sol-gel, ion exchange). 

Workflow

Example workflow

The interactive workflow panel below showcases example workflows for this solution. Each Chemspeed tool or module performs a set of specific actions, as in any manual lab workflow, and an almost limitless arrangement of these tools is possible.

MULTIPLANT / AUTOPLANT PRECIP

Details
đź’ˇ Click on a workflow node to see more details in this details panel.
Benefits

Powerful advantages

Each reactor with its own set of conditions - individually controlled tank reactors (reactor volumes 100, 240, 1’000 mL total volume) with precise, continuous feeds:

  • Up to 36 oxide syntheses per run on an AUTOPLANT, up to 6 per run on a MULTIPLANT.
  • Independent control of all process parameters in each reactor with PAT like PSD, pH.
  • Independent, precise temperature and stirring control in each reactor.
  • Up to 8 independent liquid feeds per reactor.
  • pH measurement and control (e.g. swinging pH control via acid and base).
  • Vessel-to-vessel transfer for multistep processes.
  • Gravimetric solid and viscous liquid dispensing.
  • 4-Needle Head for volumetric liquid handling and sampling.
  • Feeding and sampling under reaction conditions.
  • Cleaning in place (e.g. automated cleaning, inserts).
  • Dispensed amount, stirrer speed, temperature, pressure, time, ... and other data are stored in a read only log file.
  • Easy access to data with a convenient interface to pull results into Excel or virtually any other software.
  • Interface to DOE.
  • Exemplary integrated online benchtop XRD such as Bruker D6 Phaser, Malvern Aeris, incl.
    •  XRD device
    • Sample handover station
    • Software and hardware integration
Software

AUTOSUITE

Chemspeed’s AUTOSUITE software packages execute and control all modules in every solution. They control all Chemspeed robotic platforms and any other integrated 3rd-party software and hardware.

Explore AUTOSUITE
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Automate and digitalize your laboratory with Chemspeed.