example solution
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High output porous materials synthesis, work-up, analysis

MULTIPLANT / AUTOPLANT ZEO for porous materials synthesis
Two blue chemspeed robotic platforms in metal sitting in a white hallway
Overview

Chemspeed's solution

The leading technology in overhead gravimetric dispensing / dosing (patented) combined with our quality by design reactor technology and process excellence and user-friendly software enable you to accelerate, standardize and digitalize your porous materials (zeolites, metallorganic framework / MOF) synthesis and work-up workflows. 


Workflow

Example workflow

MULTIPLANT / AUTOPLANT ZEO

Benefits

Powerful advantages

Each reactor with its own set of conditions - individually controlled tank reactors (reactor volumes 100, 240, 1’000 mL total volume) with precise, continuous feeds:

  • Up to 12 / 24 hydro- / solvothermal syntheses per run on an AUTOPLANT (incl reaction prep, reaction execution, work-up, analysis), up to 6 per run on a semi-automated MULTIPLANT.
  • Easily exchangeable stirrer designs (anchor, twisted blade, gas entrainment stirrers…).
  • Powerful mixing for viscosities up to 80 Pa.s at 300 rpm and 30 Pa.s at 900 rpm with an anchor stirrer.
  • Independent control of all process parameters in each reactor.
  • Independent, precise temperature and stirring control in each reactor.
  • Gravimetric solid and viscous liquid dispensing.
  • 4-Needle Head for volumetric liquid handling and sampling.
  • Liquid and slurry feeds at reaction conditions.
  • Cleaning in place (e.g. automated cleaning, inserts).
  • Ventilated hood for safety and conditioned operation.
  • AUTOSUITE SOFTWARE - drag & drop experimentation with easy interface (e.g. python custom device) to e.g. LIMS, ELN, data analysis, AI / ML closed loop.
  • Optional integrated online benchtop XRD such as Bruker D6 Phaser, Malvern Aeris, incl. XRD device, sample handover station, software and hardware integration
Software
Chemspeed AutoSuite Software laptop screen